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Publications

Publications by CAP

2021

Giant Displacement Sensitivity Using Push-Pull Method in Interferometry

Authors
Robalinho, P; Frazao, O;

Publication
PHOTONICS

Abstract
We present a giant sensitivity displacement sensor combining the push-pull method and enhanced Vernier effect. The displacement sensor consists in two interferometers that are composed by two cleaved standard optical fibers coupled by a 3 dB coupler and combined with a double-sided mirror. The push pull-method is applied to the mirror creating a symmetrical change to the length of each interferometer. Furthermore, we demonstrate that the Vernier effect has a maximum sensitivity of two-fold that obtained with a single interferometer. The combination of the push-pull method and the Vernier effect in the displacement sensors allows a sensitivity of 60 +/- 1 nm/mu m when compared with a single interferometer working in the same free spectral range. In addition, exploring the maximum performance of the displacement sensors, a sensitivity of 254 +/- 6 nm/mu m is achieved, presenting a M-factor of 1071 and M-Vernier of 1.9 corresponding to a resolution of 79 pm. This new solution allows the implementation of giant-sensitive displacement measurement for a wide range of applications.

2021

Thermally Stimulated Desorption Optical Fiber-Based Interrogation System: An Analysis of Graphene Oxide Layers' Stability

Authors
Raposo, M; Xavier, C; Monteiro, C; Silva, S; Frazao, O; Zagalo, P; Ribeiro, PA;

Publication
PHOTONICS

Abstract
Thin graphene oxide (GO) film layers are being widely used as sensing layers in different types of electrical and optical sensor devices. GO layers are particularly popular because of their tuned interface reflectivity. The stability of GO layers is fundamental for sensor device reliability, particularly in complex aqueous environments such as wastewater. In this work, the stability of GO layers in layer-by-layer (LbL) films of polyethyleneimine (PEI) and GO was investigated. The results led to the following conclusions: PEI/GO films grow linearly with the number of bilayers as long as the adsorption time is kept constant; the adsorption kinetics of a GO layer follow the behavior of the adsorption of polyelectrolytes; and the interaction associated with the growth of these films is of the ionic type since the desorption activation energy has a value of 119 +/- 17 kJ/mol. Therefore, it is possible to conclude that PEI/GO films are suitable for application in optical fiber sensor devices; most importantly, an optical fiber-based interrogation setup can easily be adapted to investigate in situ desorption via a thermally stimulated process. In addition, it is possible to draw inferences about film stability in solution in a fast, reliable way when compared with the traditional ones.

2021

Acoustic Optical Fiber Sensor Based on Graphene Oxide Membrane

Authors
Monteiro, CS; Raposo, M; Ribeiro, PA; Silva, SO; Frazao, O;

Publication
SENSORS

Abstract
A Fabry-Perot acoustic sensor based on a graphene oxide membrane was developed with the aim to achieve a faster and simpler fabrication procedure when compared to similar graphene-based acoustic sensors. In addition, the proposed sensor was fabricated using methods that reduce chemical hazards and environmental impacts. The developed sensor, with an optical cavity of around 246 mu m, showed a constant reflected signal amplitude of 6.8 +/- 0.1 dB for 100 nm wavelength range. The sensor attained a wideband operation range between 20 and 100 kHz, with a maximum signal-to-noise ratio (SNR) of 32.7 dB at 25 kHz. The stability and sensitivity to temperatures up to 90 degrees C was also studied. Moreover, the proposed sensor offers the possibility to be applied as a wideband microphone or to be applied in more complex systems for structural analysis or imaging.

2021

Optical Vernier Effect: Recent Advances and Developments

Authors
Gomes, AD; Bartelt, H; Frazao, O;

Publication
LASER & PHOTONICS REVIEWS

Abstract
The optical analog of the Vernier effect applied to fiber interferometers is a recent tool to enhance the sensitivity and resolution of optical fiber sensors. This effect relies on the overlap between the signals of two interferometers with slightly detuned interference frequencies. The Vernier envelope modulation generated at the output spectrum presents magnified sensing capabilities (i.e., magnified wavelength shift) compared to that of the individual sensing interferometers that constitute the system, leading to a new generation of highly sensitive fiber sensing devices. This review analyses the recent advances and developments of the optical Vernier effect from a fiber sensing point-of-view. Initially, the fundamentals of the effect are introduced, followed by an extensive review on the state-of-the-art, presenting all the different configurations and types of fiber sensing interferometers used to introduce the optical Vernier effect. This paper also includes an overview of the complex case of enhanced Vernier effect and the introduction of harmonics to the effect.

2021

Optical Fiber Sensors for Structural Monitoring in Power Transformers

Authors
Monteiro, CS; Rodrigues, AV; Viveiros, D; Linhares, C; Mendes, H; Silva, SO; Marques, PVS; Tavares, SMO; Frazao, O;

Publication
SENSORS

Abstract
Power transformers are central elements of power transmission systems and their deterioration can lead to system failures, causing major disruptions in service. Catastrophic failures can occur, posing major environmental hazards due to fires, explosions, or oil spillage. Early fault detection can be accomplished or estimated using electrical sensors or a chemical analysis of oil or gas samples. Conventional methods are incapable of real-time measurements with a low electrical noise due to time-consuming analyses or susceptibility to electromagnetic interference. Optical fiber sensors, passive elements that are immune to electromagnetic noise, are capable of structural monitoring by being enclosed in power transformers. In this work, optical fiber sensors embedded in 3D printed structures are studied for vibration monitoring. The fiber sensor is encapsulated between two pressboard spacers, simulating the conditions inside the power transformer, and characterized for vibrations with frequencies between 10 and 800 Hz, with a constant acceleration of 10 m/s(2). Thermal aging and electrical tests are also accomplished, aiming to study the oil compatibility of the 3D printed structure. The results reported in this work suggest that structural monitoring in power transformers can be achieved using optical fiber sensors, prospecting real-time monitoring.

2021

Application of a Fiber Optic Refractometric Sensor to Measure the Concentration of Paracetamol in Crystallization Experiments

Authors
Soares, L; Cruz, P; Novais, S; Ferreira, A; Frazao, O; Silva, S;

Publication
IEEE INSTRUMENTATION & MEASUREMENT MAGAZINE

Abstract
A refractometric sensor was applied to measure in real-time the concentration of Active Pharmaceutical Ingredients (APIs) in crystallization experiments. Paracetamol was used as a model system due to the extensive literature available for this API. The refractometric sensor was fabricated by a simple and inexpensive method that consisted in splicing a short section of a multimode fiber to a single mode fiber. The compact geometry of this sensor, with an external diameter of just $125\ \mu\mathrm{m}$, allowed it to measure the concentration of paracetamol, both in a stirred tank crystallizer operating in batch and in an oscillatory flow crystallizer operating continuously. The proposed technique shows the potential to monitor the concentration of APIs in crystallizers of different sizes and geometries as an alternative to more expensive and complex analysis equipment.

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