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Publications

Publications by CAP

2024

Integrated All-In-Silica Optofluidic Platform Based on Microbubble Resonator and Femtosecond Laser Written Surface Waveguide

Authors
Amorim, VA; Frigenti, G; Baldini, F; Berneschi, S; Farnesi, D; Jorge, PAS; Maia, JM; Conti, GN; dos Santos, PSS; Marques, PVS;

Publication
IEEE SENSORS JOURNAL

Abstract
Optical microbubble resonators (OMBRs)-understood as localized thin wall bulges induced in silica microcapillaries-are gaining an ever-growing interest in microfluidic sensing applications due to their capability to sustain whispering gallery modes (WGMs) and confine the fluidic sample within their own hollow-core microcavity. Currently, most applications use an external tapered optical fiber for coupling light to the resonator. This arrangement is known to be fragile and prone to vibrations. In this work, an alternative approach, based on coupling OMBR with a femtosecond (fs) laser-written optical waveguides, integrated at the surface of fused silica substrate, is proposed. In this configuration, a stable and robust final structure is accomplished by gluing the two ends of the microcapillary, on which the OMBR is made, to the substrate. The OMBR quality factors, measured at the excitation wavelength of 1540 nm, show values close to 10(4) in the case of a water-filled cavity, with a maximum coupling efficiency of up to 6.5%. Finally, the operation of the integrated optical devices as refractometers is demonstrated by delivering different solutions with successively increasing concentrations of NaCl inside the OMBR. An average sensitivity of 45 nm/RIU is obtained, yielding a resolution of 4.4x10(-5) RIU, creating the potential for this platform to be applied in chemical/biochemical sensing.

2024

Augmented Reality for Spectral Imaging Applications

Authors
Cavaco, R; Lopes, T; Jorge, PAS; Silva, NA;

Publication
UNCONVENTIONAL OPTICAL IMAGING IV

Abstract
Spectral imaging is a technique that captures spectral information from a scene and maps it onto a 2D image, featuring the potential to reveal hidden features and properties of objects that are invisible to the human eye, such as elemental and molecular compositions. Augmented reality (AR), on the other hand, is a technology that enhances the perception of reality by superimposing digital information on the physical world. While these technologies have different purposes, they can be considered one and the same in terms of providing an user-centric extension of reality. Spectral imaging provides the information that can reveal the underlying nature of objects, while AR provides the method of visualization that can display the information in an intuitive and interactive way. In this work, we present a novel Unity toolkit that combines spectral imaging and a HoloLens 2 AR device to create an interactive and immersive experience for the user. The toolkit enables the interactive visualization of various elemental maps of a 3D rock model in AR using a simple and intuitive interface. With this technique, the user can select a sample model and an elemental map from a preloaded asset library and then see the map projected onto the rock model in AR, using simple interactions such as zoom adjustment, rotation, and pan of the models to explore features and properties in detail. The toolkit offers several advantages, including better contextual interpretation of the spectral data by placing it in relation to the shape and texture of the rock, increased user engagement and curiosity through the creation of a realistic and immersive experience, and ease of decision-making through the provision of comparative tools. In short, by combining spectral imaging and AR, we present an innovative approach that can enrich the user experience and expand the user knowledge of the environment.

2024

Automated Optical Tweezers for Enhanced Bioparticle Analysis via Combined Scattering and Raman Spectroscopy

Authors
Teixeira, J; Ribeiro, J; Silva, N; Jorge, P;

Publication
2024 IEEE SENSORS APPLICATIONS SYMPOSIUM, SAS 2024

Abstract
This paper describes the development of an optical tweezers system that operates in fully automatic mode. It features image recognition for particle tracking, allowing for the optical trapping and analysis of identified targets. The system can perform analysis of forward scattered light and Raman spectroscopy of the trapped particles, facilitating the automated analysis of a large number of samples without manual intervention. By leveraging combined analytical methods and AI for robust classification, this system contributes to the advancement of automated diagnostic tools. Preliminary results demonstrate the system's effectiveness using different kinds of standard and biofunctionalized PMMA microparticles.

2024

Linear Fiber Laser Configurations for Optical Concentration Sensing in Liquid Solutions

Authors
Soares, L; Perez-Herrera, RA; Novais, S; Ferreira, A; Silva, S; Frazao, O;

Publication
PHOTONICS

Abstract
In this study, different configurations based on linear fiber lasers were proposed and experimentally demonstrated to measure the concentration of liquid solutions. Samples of paracetamol liquid solutions with different concentrations, in the range from 52.61 to 201.33 g/kg, were used as a case-study. The optical gain was provided by a commercial bidirectional Erbium-Doped Fiber Amplifier (EDFA) and the linear cavity was obtained using two commercial Fiber Bragg Gratings (FBGs). The main difference of each configuration was the coupling ratio of the optical coupler used to extract the system signal. The sensing head corresponded to a Single-Mode Fiber (SMF) tip that worked as an intensity sensor. The results reveal that, despite the optical coupler used (50:50, 60:40, 70:30 or 80:20), all the configurations reached the laser condition, however, the concentration sensing was only possible using a laser drive current near to the threshold value. The configurations using a 70:30 and an 80:20 optical coupler allowed paracetamol concentration measurements with a higher sensitivity of (-3.00 +/- 0.24) pW/(g/kg) to be performed. In terms of resolution, the highest value obtained was 1.75 g/kg, when it was extracted at 20% of the output power to the linear cavity fiber laser configuration.

2024

Enhanced Sensitivity in Optical Sensors through Self-Image Theory and Graphene Oxide Coating

Authors
Cunha, C; Monteiro, C; Vaz, A; Silva, S; Frazao, O; Novais, S;

Publication
SENSORS

Abstract
This paper presents an approach to enhancing sensitivity in optical sensors by integrating self-image theory and graphene oxide coating. The sensor is specifically engineered to quantitatively assess glucose concentrations in aqueous solutions that simulate the spectrum of glucose levels typically encountered in human saliva. Prior to sensor fabrication, the theoretical self-image points were rigorously validated using Multiphysics COMSOL 6.0 software. Subsequently, the sensor was fabricated to a length corresponding to the second self-image point (29.12 mm) and coated with an 80 mu m/mL graphene oxide film using the Layer-by-Layer technique. The sensor characterization in refractive index demonstrated a wavelength sensitivity of 200 +/- 6 nm/RIU. Comparative evaluations of uncoated and graphene oxide-coated sensors applied to measure glucose in solutions ranging from 25 to 200 mg/dL showed an eightfold sensitivity improvement with one bilayer of Polyethyleneimine/graphene. The final graphene oxide-based sensor exhibited a sensitivity of 10.403 +/- 0.004 pm/(mg/dL) and demonstrated stability with a low standard deviation of 0.46 pm/min and a maximum theoretical resolution of 1.90 mg/dL.

2024

Optimizing Graphene Oxide Saturable Absorbers for Short Pulse Generation in Fiber Lasers: Characterization and Aging Assessment

Authors
Monteiro, CS; Perez-Herrera, RA; Silva, NA; Silva, SO; Frazao, O;

Publication
FIBER LASERS AND GLASS PHOTONICS: MATERIALS THROUGH APPLICATIONS IV

Abstract
The generation of short pulses in fiber lasers using saturable absorbers made of graphene oxide (GO), focusing on film thickness, was studied and optimized. The saturable absorber comprised a GO thin film deposited onto a single-mode fiber using the spray coating technique. Water-dispersed GO with a concentration of 4 mg/mL, characterized by a high proportion of monolayer flakes, was employed. This thin film was integrated into a cavity ring laser featuring an erbium-doped fiber amplifier (EDFA), resulting in a fiber laser emitting at a central emission wavelength of approximately 1564 nm and having a total cavity length of approximately 120 m. By controlling intracavity polarization, short-pulsed light was generated through mode-locking, Q switching, or a combination of both regimes. This work presents a comprehensive characterization of the cavity ring laser operating under the mode-locking regime. It encompasses an analysis of the spectral behavior, focusing on the evolution of the Kelly's sidebands with increasing pump power, as well as an assessment of its temporal stability. Moreover, the effects of the aging of the saturable absorber material were studied after a time period of 6 months after the fabrication. It was observed that the general characteristics of spectral signal of the laser were maintained, with long-term stability .

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