2024
Authors
Monteiro, CS; Perez-Herrera, RA; Silva, NA; Silva, SO; Frazao, O;
Publication
FIBER LASERS AND GLASS PHOTONICS: MATERIALS THROUGH APPLICATIONS IV
Abstract
The generation of short pulses in fiber lasers using saturable absorbers made of graphene oxide (GO), focusing on film thickness, was studied and optimized. The saturable absorber comprised a GO thin film deposited onto a single-mode fiber using the spray coating technique. Water-dispersed GO with a concentration of 4 mg/mL, characterized by a high proportion of monolayer flakes, was employed. This thin film was integrated into a cavity ring laser featuring an erbium-doped fiber amplifier (EDFA), resulting in a fiber laser emitting at a central emission wavelength of approximately 1564 nm and having a total cavity length of approximately 120 m. By controlling intracavity polarization, short-pulsed light was generated through mode-locking, Q switching, or a combination of both regimes. This work presents a comprehensive characterization of the cavity ring laser operating under the mode-locking regime. It encompasses an analysis of the spectral behavior, focusing on the evolution of the Kelly's sidebands with increasing pump power, as well as an assessment of its temporal stability. Moreover, the effects of the aging of the saturable absorber material were studied after a time period of 6 months after the fabrication. It was observed that the general characteristics of spectral signal of the laser were maintained, with long-term stability .
2024
Authors
Cunha, C; Monteiro, C; Vaz, A; Silva, S; Frazao, O; Novais, S;
Publication
OPTICAL SENSING AND DETECTION VIII
Abstract
This work provides a method that combines graphene oxide coating and self-image theory to improve the sensitivity of optical sensors. The sensor is designed specifically to measure the amount of glucose present quantitatively in aqueous solutions that replicate the range of glucose concentrations found in human saliva. COMSOL Multiphysics 6.0 was used to simulate the self-imaging phenomenon using a coreless silica fiber (CSF). For high-quality self-imaging, the second and fourth self-imaging points are usually preferred because of their higher coupling efficiency, which increases the sensor sensitivity. However, managing the fourth self-image is more difficult because it calls for a longer CSF length. As a result, the first and second self-image points were the focus of the simulation in this work. After the simulation, using the Layerby-Layer method, the sensor was constructed to a length that matched the second self-image point (29.12 mm) and coated with an 80 mu m/mL graphene oxide layer. When comparing uncoated and graphene oxide-covered sensors to measure glucose in liquids ranging from 25 to 200 mg/dL, one bilayer of polyethyleneimine/graphene demonstrated an eight-fold improvement in sensitivity. The final sensor, built on graphene oxide, showed stability with a low standard deviation of 0.6 pm/min. It also showed sensitivity at 10.403 +/- 0.004 pm/(mg/dL) with a limit of detection of 9.15 mg/dL.
2024
Authors
Cunha, C; Silva, S; Frazao, O; Novais, S;
Publication
EOS ANNUAL MEETING, EOSAM 2024
Abstract
Raman technology offers a cutting-edge approach to measuring glucose solutions, providing precise and non-invasive analysis. By probing the vibrational energy levels of molecular bonds, Raman technology generates a unique spectral fingerprint that allows for the accurate determination of glucose concentrations. This study proposes the use of Raman spectroscopy to identify different glucose concentrations through the detection of Raman fingerprints. As expected, higher concentrations of glucose in the solution conducted to higher peak bands, indicating more glucose molecules interacting with light and consequently increasing the magnitude of inelastic scattering. This non-destructive approach preserves sample integrity and facilitates rapid analysis, making it suitable for various applications in biomedical research, pharmaceutical development, and food science.
2024
Authors
Robalinho, P; Rodrigues, A; Novais, S; Ribeiro, ABL; Silva, S; Frazao, O;
Publication
EOS ANNUAL MEETING, EOSAM 2024
Abstract
This work proposes a signal processing algorithm to analyse the optical signal from a Low Coherence Interferometric (LCI) system. The system uses a Mach-Zehnder (MZ) interferometer to interrogate a Fabry-Perot cavity, working as an optical sensor. This algorithm is based on the correlation and convolution operations, which allows the signal to be reconstructed based on itself, as well as, on the linearization of the signal phase, allowing the non-linearities of the actuator incorporated on the MZ interferometer to be compensated. The results show a noise reduction of 30 dB in the signal acquired. As a result, a reduction of 8.2 dB in the uncertainty of the measurement of the physical measurand is achieved. It is also demonstrated that the phase linearization made it possible to obtain a coefficient of determination (namely, R-squared) higher than 0.999.
2024
Authors
Soares, L; Novais, S; Ferreira, A; Frazao, O; Silva, S;
Publication
EOS ANNUAL MEETING, EOSAM 2024
Abstract
Optical fiber sensors were implemented to measure in-situ temperature variations in an oscillatory flow crystallizer operating in continuous. The sensors were fabricated by cleaved in the middle 8 mm-length fiber Bragg gratings, forming tips with a Bragg grating of 4 mm inscribed at the fiber ends. The geometry of the sensors fabricated, with a diameter of 125 mu m, allowed the temperature monitorization of the process flow, inside the crystallizer, at four different points: input, two intermediate points, and output. The results revealed that the proposed technology allows to perform an in-situ and in line temperature monitorization, during all the crystallization process, as an alternative to more expensive and complex technology.
2024
Authors
Robalinho, P; Rodrigues, AV; Novais, S; Ribeiro, AL; Silva, S; Frazao, O;
Publication
IEEE SENSORS JOURNAL
Abstract
The aim of this work is to introduce a novel digital signal processing method for data acquired using low coherence interferometry (LCI) with a 1-kHz actuator oscillation frequency. Convolution and correlation operations are employed as efficient filters, reducing computational complexity for multilayer filtering. An envelope filtering technique is developed to address discrepancies in peak signal determination caused by nonlinear actuator motion. Additionally, a phase linearization method is presented to normalize the peak position relative to the actuator signal. Experimental results demonstrate a significant signal-to-noise ratio (SNR) improvement of 50 dB. Long-term measurements reveal an 11-dB noise reduction for frequencies below 1 mHz. This research enables LCI implementation at sampling rates of at least 1 kHz and expands its applicability to extreme measurement conditions.
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