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Publications

Publications by Susana Oliveira Silva

2021

Application of a Fiber Optic Refractometric Sensor to Measure the Concentration of Paracetamol in Crystallization Experiments

Authors
Soares, L; Cruz, P; Novais, S; Ferreira, A; Frazao, O; Silva, S;

Publication
IEEE INSTRUMENTATION & MEASUREMENT MAGAZINE

Abstract
A refractometric sensor was applied to measure in real-time the concentration of Active Pharmaceutical Ingredients (APIs) in crystallization experiments. Paracetamol was used as a model system due to the extensive literature available for this API. The refractometric sensor was fabricated by a simple and inexpensive method that consisted in splicing a short section of a multimode fiber to a single mode fiber. The compact geometry of this sensor, with an external diameter of just $125\ \mu\mathrm{m}$, allowed it to measure the concentration of paracetamol, both in a stirred tank crystallizer operating in batch and in an oscillatory flow crystallizer operating continuously. The proposed technique shows the potential to monitor the concentration of APIs in crystallizers of different sizes and geometries as an alternative to more expensive and complex analysis equipment.

2021

Environmental Sensitivity of Fabry-Perot Microcavities Induced by Layered Graphene-Dielectric Hybrid Coatings

Authors
Peixoto, R; Pires, JPS; Monteiro, CS; Raposo, M; Ribeiro, PA; Silva, SO; Frazao, O; Lopes, JMVP;

Publication
PHYSICAL REVIEW APPLIED

Abstract
We propose a fiber-based environmental sensor that exploits the reflection-phase-shift tunability provided by the use of layered coatings composed of dielectric slabs spaced by conducting membranes. A transfer-matrix study is done in a simplified theoretical model, for which an enhanced sensitivity of the reflection interference pattern to the output medium is demonstrated, in the typical refractive index range of liquid media. An experimental configuration using a cascaded Fabry-Perot microcavity coated by a graphene oxide/polyethylenimine (GO/PEI) multilayered structure is demonstrated. Its cost-effective chemical production method makes graphene oxide-based hybrid coatings excellent candidates for future real-life sensing devices.

2021

Characterization of an hollow core PCF for endoscopy applications: A proof concept

Authors
Marques J.; Novais S.; Silva S.; Frazao O.;

Publication
2021 Telecoms Conference, ConfTELE 2021

Abstract
Two distinct optical fibers for endoscope-based configurations are demonstrated and studied in this work. The fibers used for the experiment consist of: a conventional singlemode fiber (SMF 28e) and a hollow core photonic crystal fiber (HC-PCF) based on silica. Two studies that allowed the characterization of these fibers, according to their optical output power and when subjected to curvature, were carried out. The intensity power profile was also analysed in relation to the propagation distance, transversal displacement and incidence angle. After this study it can be concluded that the most suitable solution for the endoscope is the HC-PCF fiber working as a transmission probe. For the proof of concept of the fiber-based endoscope, a cleaved multimode fiber (MMF) tip was used as a reception probe and its reflection efficiency was also analysed.

2022

Sputtering Deposition of TiO2 Thin Film Coatings for Fiber Optic Sensors

Authors
Silva, D; Monteiro, CS; Silva, SO; Frazao, O; Pinto, JV; Raposo, M; Ribeiro, PA; Serio, S;

Publication
PHOTONICS

Abstract
Thin films of titanium dioxide (TiO2) and titanium (Ti) were deposited onto glass and optical fiber supports through DC magnetron sputtering, and their transmission was characterized with regard to their use in optical fiber-based sensors. Deposition parameters such as oxygen partial pressure, working pressure, and sputtering power were optimized to attain films with a high reflectance. The films deposited on glass supports were characterized by UV-Vis spectroscopy, X-ray diffraction (XRD), and scanning electron microscopy (SEM). Regarding the deposition parameters, all three parameters were tested simultaneously, changing the working pressure, the sputtering power, and the oxygen percentage. It was possible to conclude that a lower working pressure and higher applied power lead to films with a higher reflectance. Through the analysis of the as-sputtered thin films using X-ray diffraction, the deposition of both Ti and TiO2 films was confirmed. To study the applicability of TiO2 and Ti in fiber sensing, several thin films were deposited in single mode fibers (SMFs) using the sputtering conditions that revealed the most promising results in the glass supports. The sputtered TiO2 and Ti thin films were used as mirrors to increase the visibility of a low-finesse Fabry-Perot cavity and the possible sensing applications were studied.

2022

A Brief Review on Optical Fiber Sensing for the Power Grid

Authors
Rodrigues, AV; Monteiro, C; Silva, SO; Linhares, C; Mendes, H; Tavares, SMO; Frazão, O;

Publication
U.Porto Journal of Engineering

Abstract
In this work, a brief review on the application of fiber optic sensors on power grid apparatus is presented. Power transformers, which are the nodes between electrical transmission lines, are the most expensive, critical and one of the central units of this network. The failure of electrical machines compromises the whole grid leading to power outages and income losses. Thus, constant monitoring of structural health and operating conditions of core infrastructures is sought. With different types of sensors either on the market or in the literature, it is possible to measure physical parameters that make this equipment more reliable. © 2022, Universidade do Porto - Faculdade de Engenharia. All rights reserved.

2020

Graphene oxide diaphragm for acoustic fiber sensing

Authors
Monteiro, CS; Silva, SO; Santos, JL; Frazao, O;

Publication
Optics InfoBase Conference Papers

Abstract
A fiber sensor composed by a graphene oxide membrane at the tip of a capillary is presented. The graphene oxide membrane acts as a low-reflectivity mirror, distanced from a single mode fiber forming a low finesse Fabry-Perot interferometer. The response of the sensor to acoustic pressure with varying frequency is studied in the range between 5 and 45 kHz, attaining a minimum signal to noise ratio of 14 dB. © 2021 The Author(s).

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