Cookies Policy
The website need some cookies and similar means to function. If you permit us, we will use those means to collect data on your visits for aggregated statistics to improve our service. Find out More
Accept Reject
  • Menu
Publications

Publications by PHT

2021

Unravelling Plant-Pathogen Interactions: Proximal Optical Sensing as an Effective Tool for Early Detect Plant Diseases

Authors
Reis-Pereira, M; Martins, RC; Silva, AF; Tavares, F; Santos, F; Cunha, M;

Publication
Chemistry Proceedings

Abstract
This study analyzed the potential of proximal optical sensing as an effective approach for early disease detection. A compact, modular sensing system, combining direct UV–Vis spectroscopy with optical fibers, supported by a principal component analysis (PCA), was applied to evaluate the modifications promoted by the bacteria Xanthomonas euvesicatoria in tomato leaves (cv. cherry). Plant infection was achieved by spraying a bacterial suspension (108 CFU mL-1) until run-off occurred, and a similar approach was followed for the control group, where only water was applied. A total of 270 spectral measurements were performed on leaves, on five different time instances, including pre- and post-inoculation measurements. PCA was then applied to the acquired data from both healthy and inoculated leaves, which allowed their distinction and differentiation, three days after inoculation, when unhealthy plants were still asymptomatic.

2021

Thermally Stimulated Desorption Optical Fiber-Based Interrogation System: An Analysis of Graphene Oxide Layers' Stability

Authors
Raposo, M; Xavier, C; Monteiro, C; Silva, S; Frazao, O; Zagalo, P; Ribeiro, PA;

Publication
PHOTONICS

Abstract
Thin graphene oxide (GO) film layers are being widely used as sensing layers in different types of electrical and optical sensor devices. GO layers are particularly popular because of their tuned interface reflectivity. The stability of GO layers is fundamental for sensor device reliability, particularly in complex aqueous environments such as wastewater. In this work, the stability of GO layers in layer-by-layer (LbL) films of polyethyleneimine (PEI) and GO was investigated. The results led to the following conclusions: PEI/GO films grow linearly with the number of bilayers as long as the adsorption time is kept constant; the adsorption kinetics of a GO layer follow the behavior of the adsorption of polyelectrolytes; and the interaction associated with the growth of these films is of the ionic type since the desorption activation energy has a value of 119 +/- 17 kJ/mol. Therefore, it is possible to conclude that PEI/GO films are suitable for application in optical fiber sensor devices; most importantly, an optical fiber-based interrogation setup can easily be adapted to investigate in situ desorption via a thermally stimulated process. In addition, it is possible to draw inferences about film stability in solution in a fast, reliable way when compared with the traditional ones.

2021

Mach-Zehnder Interferometer-Based Evanescent Refractometer Inscribed at the Surface of Eagle2000 by Femtosecond Laser Writing

Authors
Amorim, VA; Maia, JM; Viveiros, D; Marques, PVS;

Publication
IEEE SENSORS JOURNAL

Abstract
The potential of evanescent Mach-Zehnder interferometers, embedded in Eagle2000 substrates, as refractive index sensors was assessed. For that, femtosecond laser direct writing and wet etching were used to fabricate and expose the sensing arm at the surface of the glass substrate, while keeping the reference arm buried. From the analysis of the structures' spectral response, we found that the wavelength shift of the different order peaks increased greatly for refractive indices nearing that of the glass, indicating a greater overlap between the guided mode's evanescent field and the external medium. Therefore, a maximum sensitivity of 10271 nm/RIU was obtained at a refractive index of 1.491. The sensitivity in the refractive index range of water-based solutions was, on the other hand, limited to 446 +/- 39 nm/RIU. Due to the geometry of the device, applications with films deposited at the surface of the substrate and PDMS based microfluidic channels can be explored.

2021

Turn Around Point Long Period Fiber Gratings With Coupling to Asymmetric Cladding Modes Fabricated by a Femtosecond Laser and Coated With Titanium Dioxide

Authors
Viveiros, D; de Almeida, JMMM; Coelho, L; Vasconcelos, H; Maia, JM; Amorim, VA; Jorge, PAS; Marques, PVS;

Publication
JOURNAL OF LIGHTWAVE TECHNOLOGY

Abstract
A detailed study of turn around point (TAP) long period fiber gratings (LPFGs) with coupling to the asymmetric cladding modes of a standard single-mode fiber (SMF-28e), fabricated by femtosecond (fs) laser direct writing was realized. The entire fabrication process, including the coating with different titanium dioxide (TiO2) film thicknesses of LPFGs and the corrections needed to achieve coated devices operating precisely in the TAP condition with coupling to the asymmetric cladding modes, was addressed. The significant fabrication details are also given, such as inscription periods, shape and localization of the refractive index modifications across the core. The fabrication process described allows the optimization of the LPFGs sensitivity in regards to the surrounding refractive index (SRI). Optimization of the writing parameters to obtain gratings working at the TAP for two different media surrounding the fiber (water and air) was achieved. It was demonstrated that for a grating period of 191.8 mu m, the LP1,12 mode exhibits a TAP at 1442.7 nm in air, and for a period of 192.5 mu m, the same mode exhibits a TAP at 1448.6 nm in water. The LPFGs operating at the TAP in air and water were coated with 10, 20, and 30 nm thin TiO2 film thicknesses and the spectral behavior characterized. The wavelength sensitivity to the surrounding refractive index (SRI) was assessed in the range between 1.3700 to 1.4120, and a maximum sensitivity of similar to 8051.4 nm/RIU was measured for the 192.5 mu m LPFG coated with a 30 nm thick TiO2 film.

2021

Second-Order Dispersion Sensor Based on Multi-Plasmonic Surface Resonances in D-Shaped Photonic Crystal Fibers

Authors
Cardoso, MP; Silva, AO; Romeiro, AF; Giraldi, MTR; Costa, JCWA; Santos, JL; Baptista, JM; Guerreiro, A;

Publication
PHOTONICS

Abstract
This paper proposes a scheme to determine the optical dispersion properties of a medium using multiple localized surface plasmon resonances (SPR) in a D-shaped photonic crystal fiber (PCF) whose flat surface is covered by three adjacent gold layers of different thicknesses. Using computational simulations, we show how to customize plasmon resonances at different wavelengths, thus allowing for obtaining the second-order dispersion. The central aspect of this sensing configuration is to balance miniaturization with low coupling between the different localized plasmon modes in adjacent metallic nanostructures. The determination of the optical dispersion over a large spectral range provides information on the concentration of different constituents of a medium, which is of paramount importance when monitoring media with time-varying concentrations, such as fluidic media.

2021

Characterization and Comparison of the Relative Humidity Response of Hydromorphic Polymers in Long-Period Fiber Grating Structures

Authors
Dias, B; Mendes, JP; de Almeida, JMMM; Coelho, LCC;

Publication
Chemistry Proceedings

Abstract
Relative humidity monitorization is of extreme importance on scientific and industrial applications, and fiber optics-based sensors may provide solutions where other types of sensors have limitations. In this work, fiber optics’ sensors were fabricated by combining Long-Period Fiber Gratings with three different humidity-responding polymers, namely Poly(vinyl alcohol), Poly(ethylene glycol) and Hydromed™ D4. The performance of the multiple sensors was experimentally tested and crossed with numerical simulations, which provide a comparison with the expected response given the optical properties of the materials.

  • 15
  • 75