2022
Authors
Vasconcelos, HCASG; de Almeida, JMMM; Mendes, JP; Dias, B; Jorge, PAD; Saraiva, CMT; Coelho, LCC;
Publication
IEEE SENSORS JOURNAL
Abstract
Biogenic amines (BAs) are compounds found in a vast range of food products. In recent years, there has been a crescent awareness toward food safety, followed by an increase in food regulations. Long-period fiber gratings (LPFGs) coated with titanium dioxide (TiO2) were used to monitor the optical properties of a layer of poly(ethylene-co-vinyl acetate) (PEVA) doped with maleic anhydride (MA), which was polymerized on top of TiO2. This hydrophobic polymeric structure is permeable to BA, which causes a steady increase in its effective refractive index (RI) causing a wavelength shift in the coated LPFG attenuation band. LPFG wavelength shift was observed and measured for the monoamine tyramine (TYR), to the diamines, putrescine (PUT), cadaverine (CAD), histamine (HIS), and tryptamine (TRYP), and to the polyamines, spermidine (SPED), and spermine (SPEM). It was determined that, while PEVA-coated devices present a residual sensitivity to BA, the MA greatly increases it. In fact, for PEVA only coated LPFGs, the sensitivities of 1.45 +/- 0.11, 0.97 +/- 0.05, 0.46 +/- 0.08, and 0.94 +/- 0.09 nmM-1 for PUT, CAD, HIS, and TYR, respectively, were measured. However, for PEVA-doped MA-coated LPFGs, the sensitivities are 3.34 +/- 0.13, 3.06 +/- 0.11, 2.62 +/- 0.14, and 3.65 +/- 0.23 nmM-1 for PUT, CAD, HIS, and TYR, respectively. Thus, the RI of PEVA increases with BAs in- diffusion, and MA doping further enhances the PEVA sensitivity to BA. The proposed sensor is expected to play a part in the further development of a biosensor for the quantification of BA in real foodstuff, providing a methodology for quality control.
2020
Authors
Viveiros, D; De Almeida, JMMM; Coelho, L; Vasconcelos, H; Maia, JM; Amorim, VA; Jorge, PAS; Marques, PVS;
Publication
Optics InfoBase Conference Papers
Abstract
The fabrication of Turn Around Point Long Period Fiber Grating in standard SMF-28e fibers through femtosecond laser direct writing is demonstrated and its sensing sensitivity is improved by coating the fiber with titanium dioxide through physical vapor deposition. © 2021 The Author(s).
2020
Authors
Viveiros, D; De Almeida, JMMM; Coelho, L; Maia, JM; Amorim, VA; Jorge, PAS; Marques, PVS;
Publication
Optics InfoBase Conference Papers
Abstract
The precise production of 4.5 µm off-axis first order FBG in an SMF-28e fiber through femtosecond laser direct writing is demonstrated. The off-axis FBG potential as sensing head for torsion sensing was successfully explored. © 2021 The Author(s).
2020
Authors
Viveiros, D; Vasconcelos, H; De Almeida, JMMM; Coelho, L; Amorim, VA; Maia, JM; Jorge, PAS; Marques, PVS;
Publication
Optics InfoBase Conference Papers
Abstract
Optical fiber Mach-Zehnder interferometers were fabricated by combining two TiO2 coated LPFGs fabricated through femtosecond laser direct writing. Results of its refractometric characterization are presented and compared with the single LPFGs sensors. Wavelength sensitivity of 1175 nm/RIU at 1.38 and spectral resolution of 2.2×10-5 were achieved. © 2021 The Author(s).
2022
Authors
Vasconcelos, H; De Almeida, JMMM; Mendes, J; Dias, B; Jorge, PAS; Saraiva, C; Coelho, LCC;
Publication
Optics InfoBase Conference Papers
Abstract
Long period fiber gratings coated with TiO2 and poly(ethylene-co-vinyl acetate) (PEVA), a polymeric structure permeable biogenic amines found in foodstuff, were used to detect these compounds through the wavelength shift of its attenuation band. © 2022 The Author(s).
2022
Authors
Dias, B; de Almeida, JMM; Coelho, LCC;
Publication
EPJ Web of Conferences
Abstract
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