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Publications

Publications by Paulo Vicente Marques

2021

Mach-Zehnder Interferometer-Based Evanescent Refractometer Inscribed at the Surface of Eagle2000 by Femtosecond Laser Writing

Authors
Amorim, VA; Maia, JM; Viveiros, D; Marques, PVS;

Publication
IEEE SENSORS JOURNAL

Abstract
The potential of evanescent Mach-Zehnder interferometers, embedded in Eagle2000 substrates, as refractive index sensors was assessed. For that, femtosecond laser direct writing and wet etching were used to fabricate and expose the sensing arm at the surface of the glass substrate, while keeping the reference arm buried. From the analysis of the structures' spectral response, we found that the wavelength shift of the different order peaks increased greatly for refractive indices nearing that of the glass, indicating a greater overlap between the guided mode's evanescent field and the external medium. Therefore, a maximum sensitivity of 10271 nm/RIU was obtained at a refractive index of 1.491. The sensitivity in the refractive index range of water-based solutions was, on the other hand, limited to 446 +/- 39 nm/RIU. Due to the geometry of the device, applications with films deposited at the surface of the substrate and PDMS based microfluidic channels can be explored.

2021

Intensity-modulated refractometer based on mode-mismatch in surface waveguides inscribed by femtosecond laser direct writing

Authors
Amorim, VA; Viveiros, D; Maia, JM; Marques, PVS;

Publication
OPTICS AND LASER TECHNOLOGY

Abstract
Optical waveguides were fabricated at the surface of Eagle2000 glass substrates, using femtosecond laser direct writing and wet etching, and their potential as intensity-modulated refractometers was assessed. Through the analysis of their broadband spectral response to different refractive index oils, we observed that mode mismatch is present when the guided mode reaches the surface of the substrate and interacts with the external medium, thus enabling the use of such optical waveguides in refractive index sensing. Refractive indices equal to or greater than that of the substrate also induced a coupling mechanism that was shown not to be suitable in these devices. The device's wavelength of operation was found to be tunable by controlling the distance between the surface and the center of the optical waveguide. However, the sensitivity was seen to diminish by increasing the latter, being nonexistent for distances greater than 5.5 mu m. In this study, the maximum sensitivity values were found for a surface to core center distance between 1 and 2 mu m, in the biological range, and 2.5 to 3 mu m, for a refractive index nearing that of the substrate. Accordingly, maximum sensitivities of approximate to 25 dB/RIU and approximate to 1200 dB/RIU were found between 1.300 < n(D)(25)degrees(C) < 1.400 and 1.490 < n(D)(25)degrees(C) < 1.500, respectively.

2021

Loss mechanisms in femtosecond laser written optical waveguides

Authors
Marques, PVS; Amorim, VA; Maia, JM; Viveiros, D;

Publication
Proceedings of SPIE - The International Society for Optical Engineering

Abstract
Low loss optical waveguides are the key component for the fabrication of more complex integrated optics devices. In most works related to femtosecond laser written waveguides, the values presented give results at a single wavelength or in a narrow wavelength band; but some applications in optical sensing, for example, would benefit from waveguides having good propagation properties in a larger wavelength range. This paper presents results that allow one to gain insight into the major loss mechanisms present in laser written waveguides in two different types of glasses (fused silica and Eagle 2000 glass) and the dependence of those on the fabrication parameters. Finally, an example of application of broadband operating waveguides is given.

2021

Femtosecond laser micromachining of an optofluidics-based monolithic whispering-gallery mode resonator coupled to a suspended waveguide

Authors
Maia, JM; Amorim, VA; Viveiros, D; Marques, PVS;

Publication
SCIENTIFIC REPORTS

Abstract
A monolithic lab-on-a-chip fabricated by femtosecond laser micromachining capable of label-free biosensing is reported. The device is entirely made of fused silica, and consists of a microdisk resonator integrated inside a microfluidic channel. Whispering gallery modes are excited by the evanescent field of a circular suspended waveguide, also incorporated within the channel. Thermal annealing is performed to decrease the surface roughness of the microstructures to a nanometric scale, thereby reducing intrinsic losses and maximizing the Q-factor. Further, thermally-induced morphing is used to position, with submicrometric precision, the suspended waveguide tangent to the microresonator to enhance the spatial overlap between the evanescent field of both optical modes. With this fabrication method and geometry, the alignment between the waveguide and the resonator is robust and guaranteed at all instances. A maximum sensitivity of 121.5 nm/RIU was obtained at a refractive index of 1.363, whereas near the refractive index range of water-based solutions the sensitivity is 40 nm/RIU. A high Q-factor of 10(5) is kept throughout the entire measurement range.

2021

Turn Around Point Long Period Fiber Gratings With Coupling to Asymmetric Cladding Modes Fabricated by a Femtosecond Laser and Coated With Titanium Dioxide

Authors
Viveiros, D; de Almeida, JMMM; Coelho, L; Vasconcelos, H; Maia, JM; Amorim, VA; Jorge, PAS; Marques, PVS;

Publication
JOURNAL OF LIGHTWAVE TECHNOLOGY

Abstract
A detailed study of turn around point (TAP) long period fiber gratings (LPFGs) with coupling to the asymmetric cladding modes of a standard single-mode fiber (SMF-28e), fabricated by femtosecond (fs) laser direct writing was realized. The entire fabrication process, including the coating with different titanium dioxide (TiO2) film thicknesses of LPFGs and the corrections needed to achieve coated devices operating precisely in the TAP condition with coupling to the asymmetric cladding modes, was addressed. The significant fabrication details are also given, such as inscription periods, shape and localization of the refractive index modifications across the core. The fabrication process described allows the optimization of the LPFGs sensitivity in regards to the surrounding refractive index (SRI). Optimization of the writing parameters to obtain gratings working at the TAP for two different media surrounding the fiber (water and air) was achieved. It was demonstrated that for a grating period of 191.8 mu m, the LP1,12 mode exhibits a TAP at 1442.7 nm in air, and for a period of 192.5 mu m, the same mode exhibits a TAP at 1448.6 nm in water. The LPFGs operating at the TAP in air and water were coated with 10, 20, and 30 nm thin TiO2 film thicknesses and the spectral behavior characterized. The wavelength sensitivity to the surrounding refractive index (SRI) was assessed in the range between 1.3700 to 1.4120, and a maximum sensitivity of similar to 8051.4 nm/RIU was measured for the 192.5 mu m LPFG coated with a 30 nm thick TiO2 film.

2021

Optical Fiber Sensors for Structural Monitoring in Power Transformers

Authors
Monteiro, CS; Rodrigues, AV; Viveiros, D; Linhares, C; Mendes, H; Silva, SO; Marques, PVS; Tavares, SMO; Frazao, O;

Publication
SENSORS

Abstract
Power transformers are central elements of power transmission systems and their deterioration can lead to system failures, causing major disruptions in service. Catastrophic failures can occur, posing major environmental hazards due to fires, explosions, or oil spillage. Early fault detection can be accomplished or estimated using electrical sensors or a chemical analysis of oil or gas samples. Conventional methods are incapable of real-time measurements with a low electrical noise due to time-consuming analyses or susceptibility to electromagnetic interference. Optical fiber sensors, passive elements that are immune to electromagnetic noise, are capable of structural monitoring by being enclosed in power transformers. In this work, optical fiber sensors embedded in 3D printed structures are studied for vibration monitoring. The fiber sensor is encapsulated between two pressboard spacers, simulating the conditions inside the power transformer, and characterized for vibrations with frequencies between 10 and 800 Hz, with a constant acceleration of 10 m/s(2). Thermal aging and electrical tests are also accomplished, aiming to study the oil compatibility of the 3D printed structure. The results reported in this work suggest that structural monitoring in power transformers can be achieved using optical fiber sensors, prospecting real-time monitoring.

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