2024
Autores
Cunha, C; Monteiro, C; Vaz, A; Silva, S; Frazao, O; Novais, S;
Publicação
OPTICAL SENSING AND DETECTION VIII
Abstract
This work provides a method that combines graphene oxide coating and self-image theory to improve the sensitivity of optical sensors. The sensor is designed specifically to measure the amount of glucose present quantitatively in aqueous solutions that replicate the range of glucose concentrations found in human saliva. COMSOL Multiphysics 6.0 was used to simulate the self-imaging phenomenon using a coreless silica fiber (CSF). For high-quality self-imaging, the second and fourth self-imaging points are usually preferred because of their higher coupling efficiency, which increases the sensor sensitivity. However, managing the fourth self-image is more difficult because it calls for a longer CSF length. As a result, the first and second self-image points were the focus of the simulation in this work. After the simulation, using the Layerby-Layer method, the sensor was constructed to a length that matched the second self-image point (29.12 mm) and coated with an 80 mu m/mL graphene oxide layer. When comparing uncoated and graphene oxide-covered sensors to measure glucose in liquids ranging from 25 to 200 mg/dL, one bilayer of polyethyleneimine/graphene demonstrated an eight-fold improvement in sensitivity. The final sensor, built on graphene oxide, showed stability with a low standard deviation of 0.6 pm/min. It also showed sensitivity at 10.403 +/- 0.004 pm/(mg/dL) with a limit of detection of 9.15 mg/dL.
2024
Autores
Robalinho, P; Rodrigues, A; Novais, S; Ribeiro, AL; Silva, S; Frazao, O;
Publicação
IEEE Sensors Journal
Abstract
The aim of this work is to introduce a novel digital signal processing method for data acquired using Low Coherence Interferometry (LCI) with a 1 kHz actuator oscillation frequency. Convolution and correlation operations are employed as efficient filters, reducing computational complexity for multi-layer filtering. An envelope filtering technique is developed to address discrepancies in peak signal determination caused by non-linear actuator motion. Additionally, a phase linearization method is presented to normalize the peak position relative to the actuator signal. Experimental results demonstrate a significant signal-to-noise ratio (SNR) improvement of 50 dB. Long-term measurements reveal an 11 dB noise reduction for frequencies below 1 mHz. This research enables LCI implementation at sampling rates of at least 1 kHz and expands its applicability to extreme measurement conditions. © 2001-2012 IEEE.
2024
Autores
Rego, GM;
Publicação
Sensors
Abstract
In this paper we derived an expression that allows the determination of the thermo-optic coefficient of weakly-guiding germanium-doped silica fibers, based on the thermal behavior of optical fiber devices, such as, fiber Bragg gratings (FBGs). The calculations rely on the full knowledge of the fiber parameters and on the temperature sensitivity of FBGs. In order to validate the results, we estimated the thermo-optic coefficient of bulk GeO2 glass at 293 K and 1.55 µm to be 18.3 × 10-6 K-1. The determination of this value required to calculate a correction factor which is based on the knowledge of the thermal expansion coefficient of the fiber core, the Pockels’ coefficients (p11 = 0.125, p12 = 0.258 and p44 = -0.0662) and the Poisson ratio (? = 0.161) of the SMF-28 fiber. To achieve that goal, we estimated the temperature dependence of the thermal expansion coefficient of GeO2 and we discussed the dispersion and temperature dependence of Pockels’ coefficients. We have presented expressions for the dependence of the longitudinal and transverse acoustic velocities on the GeO2 concentration used to calculate the Poisson ratio. We have also discussed the dispersion of the photoelastic constant. An estimate for the temperature dependence of the thermo-optic coefficient of bulk GeO2 glass is presented for the 200–300 K temperature range. © 2024 by the author.
2024
Autores
Maia, JM; Marques, PVS;
Publicação
JOURNAL OF OPTICS
Abstract
The potential of ultrafast laser machining for the design of integrated optical devices in ULE (R) glass, a material known for its low coefficient of thermal expansion (CTE), is addressed. This was done through laser direct writing and characterization of optical waveguides and through the fabrication of 3D cavities inside the glass by following laser irradiation with chemical etching. Type I optical waveguides were produced and their internal loss mechanisms at 1550 nm were studied. Coupling losses lower than 0.2 dB cm-1 were obtained within a wide processing window. However, propagation loss lower than 4.2-4.3 dB cm-1 could not be realized, unlike in other glasses, due to laser-induced photodarkening. Selective-induced etching was observed over a large processing window and found to be maximum when irradiating the glass with a fs-laser beam linearly polarised orthogonally to the scanning direction, akin to what is observed in fused silica laser-machined microfluidic channels. In fact, the etching selectivity and surface roughness of laser-machined ULE (R) glass was found to be similar to that of fused silica, allowing some of the already reported microfluidic and optofluidic devices to be replicated in this low CTE glass. An example of a 3D cavity with planar-spherically convex interfaces is given. Due to the thermal properties of ULE (R) glass, these cavities can be employed as interferometers for wavelength and/or temperature referencing.
2024
Autores
Maia, JM; Marques, PVS;
Publicação
OPTICS AND LASER TECHNOLOGY
Abstract
Low-finesse Fabry-Perot interferometers (FPI) with a plano-convex geometry are fabricated in ULE (R) glass through ultrafast laser machining. With this geometry, it is possible to overcome beam divergence effects that contribute to the poor fringe visibility usually observed in 100-mu m or longer planar-planar FPIs. By replacing the planar surface with a spherical one, the diverging beam propagating through the cavity is re-focused back at the entrance of the lead-in fiber upon reflection at this curved interface, thereby balancing out the intensities of both interfering beams and enhancing the visibility. The design of a 3D shaped cavity with a spherical sidewall is only made possible through fs-laser direct writing followed by chemical etching. In this technique, the 3D volume is reduced to writing of uniformly vertically spaced 2D layers with unique geometry, which are then selectively removed during chemical etching with HF acid. The radius of curvature that maximizes fringe visibility is computed using a numerical tool that is experimentally validated. By choosing the optimal radius of curvature, uniform visibilities in the range of 0.98-1.00 are measured for interferometers produced with cavity lengths spanning from 100 to 1000 mu m.
2024
Autores
Amorim, VA; Frigenti, G; Baldini, F; Berneschi, S; Farnesi, D; Jorge, PAS; Maia, JM; Conti, GN; dos Santos, PSS; Marques, PVS;
Publicação
IEEE SENSORS JOURNAL
Abstract
Optical microbubble resonators (OMBRs)-understood as localized thin wall bulges induced in silica microcapillaries-are gaining an ever-growing interest in microfluidic sensing applications due to their capability to sustain whispering gallery modes (WGMs) and confine the fluidic sample within their own hollow-core microcavity. Currently, most applications use an external tapered optical fiber for coupling light to the resonator. This arrangement is known to be fragile and prone to vibrations. In this work, an alternative approach, based on coupling OMBR with a femtosecond (fs) laser-written optical waveguides, integrated at the surface of fused silica substrate, is proposed. In this configuration, a stable and robust final structure is accomplished by gluing the two ends of the microcapillary, on which the OMBR is made, to the substrate. The OMBR quality factors, measured at the excitation wavelength of 1540 nm, show values close to 10(4) in the case of a water-filled cavity, with a maximum coupling efficiency of up to 6.5%. Finally, the operation of the integrated optical devices as refractometers is demonstrated by delivering different solutions with successively increasing concentrations of NaCl inside the OMBR. An average sensitivity of 45 nm/RIU is obtained, yielding a resolution of 4.4x10(-5) RIU, creating the potential for this platform to be applied in chemical/biochemical sensing.
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