Cookies
O website necessita de alguns cookies e outros recursos semelhantes para funcionar. Caso o permita, o INESC TEC irá utilizar cookies para recolher dados sobre as suas visitas, contribuindo, assim, para estatísticas agregadas que permitem melhorar o nosso serviço. Ver mais
Aceitar Rejeitar
  • Menu
Publicações

Publicações por Susana Novais

2024

Linear Fiber Laser Configurations for Optical Concentration Sensing in Liquid Solutions

Autores
Soares, L; Perez-Herrera, RA; Novais, S; Ferreira, A; Silva, S; Frazao, O;

Publicação
PHOTONICS

Abstract
In this study, different configurations based on linear fiber lasers were proposed and experimentally demonstrated to measure the concentration of liquid solutions. Samples of paracetamol liquid solutions with different concentrations, in the range from 52.61 to 201.33 g/kg, were used as a case-study. The optical gain was provided by a commercial bidirectional Erbium-Doped Fiber Amplifier (EDFA) and the linear cavity was obtained using two commercial Fiber Bragg Gratings (FBGs). The main difference of each configuration was the coupling ratio of the optical coupler used to extract the system signal. The sensing head corresponded to a Single-Mode Fiber (SMF) tip that worked as an intensity sensor. The results reveal that, despite the optical coupler used (50:50, 60:40, 70:30 or 80:20), all the configurations reached the laser condition, however, the concentration sensing was only possible using a laser drive current near to the threshold value. The configurations using a 70:30 and an 80:20 optical coupler allowed paracetamol concentration measurements with a higher sensitivity of (-3.00 +/- 0.24) pW/(g/kg) to be performed. In terms of resolution, the highest value obtained was 1.75 g/kg, when it was extracted at 20% of the output power to the linear cavity fiber laser configuration.

2024

Enhanced Sensitivity in Optical Sensors through Self-Image Theory and Graphene Oxide Coating

Autores
Cunha, C; Monteiro, C; Vaz, A; Silva, S; Frazao, O; Novais, S;

Publicação
SENSORS

Abstract
This paper presents an approach to enhancing sensitivity in optical sensors by integrating self-image theory and graphene oxide coating. The sensor is specifically engineered to quantitatively assess glucose concentrations in aqueous solutions that simulate the spectrum of glucose levels typically encountered in human saliva. Prior to sensor fabrication, the theoretical self-image points were rigorously validated using Multiphysics COMSOL 6.0 software. Subsequently, the sensor was fabricated to a length corresponding to the second self-image point (29.12 mm) and coated with an 80 mu m/mL graphene oxide film using the Layer-by-Layer technique. The sensor characterization in refractive index demonstrated a wavelength sensitivity of 200 +/- 6 nm/RIU. Comparative evaluations of uncoated and graphene oxide-coated sensors applied to measure glucose in solutions ranging from 25 to 200 mg/dL showed an eightfold sensitivity improvement with one bilayer of Polyethyleneimine/graphene. The final graphene oxide-based sensor exhibited a sensitivity of 10.403 +/- 0.004 pm/(mg/dL) and demonstrated stability with a low standard deviation of 0.46 pm/min and a maximum theoretical resolution of 1.90 mg/dL.

2024

Coreless Silica Fiber Sensor based on Self-Image Theory and coated with Graphene Oxide

Autores
Cunha, C; Monteiro, C; Vaz, A; Silva, S; Frazao, O; Novais, S;

Publicação
OPTICAL SENSING AND DETECTION VIII

Abstract
This work provides a method that combines graphene oxide coating and self-image theory to improve the sensitivity of optical sensors. The sensor is designed specifically to measure the amount of glucose present quantitatively in aqueous solutions that replicate the range of glucose concentrations found in human saliva. COMSOL Multiphysics 6.0 was used to simulate the self-imaging phenomenon using a coreless silica fiber (CSF). For high-quality self-imaging, the second and fourth self-imaging points are usually preferred because of their higher coupling efficiency, which increases the sensor sensitivity. However, managing the fourth self-image is more difficult because it calls for a longer CSF length. As a result, the first and second self-image points were the focus of the simulation in this work. After the simulation, using the Layerby-Layer method, the sensor was constructed to a length that matched the second self-image point (29.12 mm) and coated with an 80 mu m/mL graphene oxide layer. When comparing uncoated and graphene oxide-covered sensors to measure glucose in liquids ranging from 25 to 200 mg/dL, one bilayer of polyethyleneimine/graphene demonstrated an eight-fold improvement in sensitivity. The final sensor, built on graphene oxide, showed stability with a low standard deviation of 0.6 pm/min. It also showed sensitivity at 10.403 +/- 0.004 pm/(mg/dL) with a limit of detection of 9.15 mg/dL.

2024

Glucose concentration detection using a low-cost Raman Spectroscopy Kit

Autores
Cunha, C; Silva, S; Frazão, O; Novais, S;

Publicação
EPJ Web of Conferences

Abstract
Raman technology offers a cutting-edge approach to measuring glucose solutions, providing precise and non-invasive analysis. By probing the vibrational energy levels of molecular bonds, Raman technology generates a unique spectral fingerprint that allows for the accurate determination of glucose concentrations. This study proposes the use of Raman spectroscopy to identify different glucose concentrations through the detection of Raman fingerprints. As expected, higher concentrations of glucose in the solution conducted to higher peak bands, indicating more glucose molecules interacting with light and consequently increasing the magnitude of inelastic scattering. This non-destructive approach preserves sample integrity and facilitates rapid analysis, making it suitable for various applications in biomedical research, pharmaceutical development, and food science.

2015

Lithium batteries temperature and strain fiber monitoring

Autores
Nascimento, M; Novais, S; Leitao, C; Fatima Domingues, MF; Alberto, N; Antunes, P; Pinto, JL;

Publicação
24TH INTERNATIONAL CONFERENCE ON OPTICAL FIBRE SENSORS

Abstract
Fiber Bragg grating sensors were attached to the surface of a rechargeable lithium battery in order to monitor its thermal and strain fluctuations through charge and different discharge C rates. During the discharge process above 1C, it were observed, a temperature and strain fluctuations of a 4.12 +/- 0.67 degrees C and 24.64 +/- 6.02 mu epsilon, respectively. In the regular charge process, a temperature and strain variation of 1.03 +/- 0.67 degrees C and 15.86 +/- 6.02 mu epsilon, were detected.

2016

Internal and External Temperature Monitoring of a Li-Ion Battery with Fiber Bragg Grating Sensors

Autores
Novais, S; Nascimento, M; Grande, L; Domingues, MF; Antunes, P; Alberto, N; Leitao, C; Oliveira, R; Koch, S; Kim, GT; Passerini, S; Pinto, J;

Publicação
SENSORS

Abstract
The integration of fiber Bragg grating (FBG) sensors in lithium-ion cells for in-situ and in-operando temperature monitoring is presented herein. The measuring of internal and external temperature variations was performed through four FBG sensors during galvanostatic cycling at C-rates ranging from 1C to 8C. The FBG sensors were placed both outside and inside the cell, located in the center of the electrochemically active area and at the tab-electrode connection. The internal sensors recorded temperature variations of 4.0 +/- 0.1 degrees C at 5C and 4.7 +/- 0.1 degrees C at 8C at the center of the active area, and 3.9 +/- 0.1 degrees C at 5C and 4.0 +/- 0.1 degrees C at 8C at the tab-electrode connection, respectively. This study is intended to contribute to detection of a temperature gradient in real time inside a cell, which can determine possible damage in the battery performance when it operates under normal and abnormal operating conditions, as well as to demonstrate the technical feasibility of the integration of in-operando microsensors inside Li-ion cells.

  • 7
  • 9