Abstract

Abstract

Abstract
Long period fiber gratings (LPFGs) were used to monitor the characteristics of copper (Cu) thin films when annealed in air atmosphere up to similar to 680 degrees C. The wavelength and the optical power shift of the resonant bands of the LPFGs when coated with the Cu thin films, were measured as a function of the annealing temperature, and were found to exhibit a different evolution comparing to a bare LPFGs. Thin films of Cu deposited on quartz (SiO2) substrates were annealed and analyzed by XRD, SEM/EDS and Raman spectroscopy, allowing to identify the formation of two distinct oxide phases at different temperatures, cuprous (Cu2O-cuprite) and cupric (CuO-tenorite) oxides, respectively. The observed features of the resonant bands of the LPFGs were found to be associated with the Cu oxide phase transitions, indicating the possibility of using LPFGs to monitor, in real time, the oxidation states of Cu thin films by following specific characteristics of the attenuation bands. In addition, LPFGs over coated with the two distinct oxidation phases of Cu were characterized for refractive index sensing in the range between 1.300 to 1.600, leading to the conclusion that the sensitivity to the refractive index of the surrounding medium of Cu coated LPFGs sensing systems can be temperature tuned.

Abstract
A study of long period fiber gratings (LPFG) over coated with iron (Fe) and subjected to oxidation in water with different sodium chloride (NaCl) concentrations is presented. The formation of iron oxides and hydroxides was monitored in real time by following the features of the LPFG attenuation band. Preliminary results show that Fe coated LPFGs can be used as sensors for early warning of corrosion in offshore and in coastal projects where metal structures made of iron alloys are in contact with sea or brackish water.

Abstract
In this work an investigation of long period fiber gratings (LPFGs) over coated with iron (Fe) thin layers with different thicknesses and subjected to oxidation in air atmosphere under controlled temperature is presented. The formation of iron oxides was monitored in real time by following the optical features of the LPFG attenuation band. The morphology of the oxide layer was further analyzed by scanning electron microscope (SEM). Preliminary results show that iron coated LPFGs can be used as sensors for early warning of corrosion in projects where metal structures made of iron alloys are in contact with atmospheric air.

Abstract
This work reports the theoretical investigation of optical fiber surface plasmon resonance sensors incorporating bimetallic layer combinations. Different metals like silver, gold, copper, and aluminum are considered to investigate the refractometric sensing properties of tapered and tip optrode phase-interrogated optical fiber plasmonic sensor structures. It is shown that the gold-silver combination, coupled to a tip optrode layout, is capable of maximizing the resolution and operation range of these sensing structures for environmental refractive index measurement.