Abstract
X-ray fluorescence spectrometry (XRF) is a rapid, non-destructive multi-elemental analytical technique used for determining elemental contents ranging from percent down to the µg/g level. Although detection limits are much higher for XRF compared to other laboratory-based methods, such as inductively coupled plasma mass spectrometry (ICP-MS), ICP-optical emission spectrometry (OES) and atomic absorption spectrometry (AAS), its portability and ease of use make it a valuable tool, especially for field-based studies. A growing necessity to monitor human exposure to toxic metals and metalloids in consumer goods, cultural products, foods and other sample types while performing the analysis in situ has led to several important developments in portable XRF technology. In this study, a new portable XRF analyzer based on the use of doubly curved crystal optics (HD Mobile®) was evaluated for detecting toxic elements in foods, medicines, cosmetics and spices used in many Asian communities. Two models of the HD Mobile® (a pre-production and a final production unit) were investigated. Performance parameters including accuracy, precision and detection limits were characterized in a laboratory setting using certified reference materials (CRMs) and standard solutions. Bias estimates for key elements of public health significance such as As, Cd, Hg and Pb ranged from - 10% to 11% for the pre-production, and - 14% to 16% for the final production model. Five archived public health samples including herbal medicine products, ethnic spices and cosmetic products were analyzed using both XRF instruments. There was good agreement between the pre-production and final production models for the four key elements, such that the data were judged to be fit-for-purpose for the majority of samples analyzed. Detection of the four key elements of interest using the HD Mobile® was confirmed using archived samples for which ICP-OES data were available based on digested sample materials. The HD Mobile® XRF units were shown to be suitable for rapid screening of samples likely to be encountered in field based studies. © 2016 Elsevier B.V.

Abstract
The integration of fiber Bragg grating (FBG) sensors in lithium-ion cells for in-situ and in-operando temperature monitoring is presented herein. The measuring of internal and external temperature variations was performed through four FBG sensors during galvanostatic cycling at C-rates ranging from 1C to 8C. The FBG sensors were placed both outside and inside the cell, located in the center of the electrochemically active area and at the tab-electrode connection. The internal sensors recorded temperature variations of 4.0 +/- 0.1 degrees C at 5C and 4.7 +/- 0.1 degrees C at 8C at the center of the active area, and 3.9 +/- 0.1 degrees C at 5C and 4.0 +/- 0.1 degrees C at 8C at the tab-electrode connection, respectively. This study is intended to contribute to detection of a temperature gradient in real time inside a cell, which can determine possible damage in the battery performance when it operates under normal and abnormal operating conditions, as well as to demonstrate the technical feasibility of the integration of in-operando microsensors inside Li-ion cells.

Abstract
A sensing system in the near infrared region has been developed for ammonia sensing based on the wavelength modulation spectroscopy (WMS) principle. The WMS is a rather sensitive technique for detecting atomic/molecular species, presenting the advantage that it can be used in the near-infrared region by using the optical telecommunications technology. In this technique, the laser wavelength and intensity were modulated by applying a sine wave signal through the injection current, which allowed the shift of the detection bandwidth to higher frequencies where laser intensity noise was typically lower. Two multi-pass cells based on free space light propagation with 160 cm and 16 cm of optical path length were used, allowing the redundancy operation and technology validation. This system used a diode laser with an emission wavelength at 1512.21 nm, where NH3 has a strong absorption line. The control of the NH3 gas sensing system, as well as acquisition, processing and data presentation was performed.

Abstract
In this study, we investigated the temperature behavior of phase-shifted long-period fiber gratings (PS-LPFGs) inscribed in two types of optical fiber: B/Ge and SMF28. The experiments were carried out from 5 to 305 K using a superconducting quantum interference device magnetometer. The average temperature sensitivity obtained of -0.43 nm/K for PS-LPFGs inscribed in the B/Ge fiber is one order of magnitude larger than for PS-LPFGs inscribed in the SMF28 fiber, in the 60-240 K range. Values ranging from -0.08 nm/K up to 0.2 nm/K were obtained in the 5-35 K temperature range, which are considerably better than previous results achieved for metal-coated FBGs and also for LPFGs inscribed in a similar B/Ge codoped fiber. Nevertheless, further work is required in order to correctly address sensor reliability.

Abstract
In this work, a Fabry-Perot cavity based on a new silica tube design is proposed. The tube presents a cladding with a thickness of similar to 14 mu m and a hollow core. The presence of four small rods, of similar to 20 mu m diameter each, placed in diametrically opposite positions ensure the mechanical stability of the tube. The cavity, formed by splicing a section of the silica tube between two sections of single mode fiber, is characterized in strain and temperature (from room temperature to 900 degrees C). When the sensor is exposed to high temperatures, there is a change in the response to strain. The influence of the thermal annealing is investigated in order to improve the sensing head performance. (C)2015 Optical Society of America

Abstract
In this work, it is proposed a technique to implement an intensity sensor based on the generation of a double-reflecting (ghost) signal in optical time domain reflectometry (OTDR). The intensity sensor is supported by a singlemode-multimode-singlemode (SMS) fiber structure combined with a fiber loop mirror (FLM). The results of the displacement sensitivity show linear behavior for both the first-reflecting and double-reflecting signals with linear slopes of approximately -4.5 dB/mm and -6 dB/mm, respectively. The displacement resolution achieved is approximate to 0.28 mm. It is also found that the system is able to read periodic displacement variations in the millisecond time scale applied to the sensing head. (c) 2015 Wiley Periodicals, Inc. Microwave Opt Technol Lett 57:1312-1315, 2015