2015
Autores
Coelho, L; Viegas, D; Santos, JL; de Almeida, JMMM;
Publicação
OPTICAL SENSORS 2015
Abstract
Monitoring the quality of high refractive index edible oils is of great importance for the human health. Uncooked edible oils in general are healthy foodstuff, olive oil in particular, however, they are frequently used for baking and cooking. High quality edible oils are made from seeds, nuts or fruits by mechanical processes. Nevertheless, once the mechanical extraction is complete, up to 15% of the oil remains in oil pomace and in the mill wastewater, which can be extracted using organic solvents, often hexane. Optical fiber sensors based on long period fiber gratings (LPFG) have very low wavelength sensitivity when the surround refractive index is higher than the refractive index of the cladding. Titanium dioxide (TiO2) coated LPFG could lead to the realization of high sensitivity chemical sensor for the food industry. In this work LPFG coated with a TiO2 thin film were successfully used for to detect small levels of hexane diluted in edible oils and for real time monitoring the thermal deterioration of edible oils. For a TiO2 coating of 30 nm a wavelength sensitivity of 1361.7 nm/RIU (or 0.97 nm /% V/V) in the 1.4610-1.4670 refractive index range was achieved, corresponding to 0 to 12 % V/V of hexane in olive oil. A sensitivity higher than 638 nm/RIU at 225 degrees C was calculated, in the 1.4670-1.4735 refractive index range with a detection limit of thermal deterioration of about 1 minute.
2015
Autores
Rota Rodrigo, S; Lopez Amo, M; Kobelke, J; Schuster, K; Santos, JL; Frazao, O;
Publicação
JOURNAL OF LIGHTWAVE TECHNOLOGY
Abstract
In this study, a multimodal interferometer based on a suspended core photonic crystal fiber (PCF) for simultaneous strain and temperature measurements is proposed. The structure is also employed for angle measurements. The sensor comprises a 3-mm-suspended core PCF between SMFs and is based on the combination of two multimodal interferences with different frequency fringe patterns. The interferometric patterns show different sensitivity responses to strain and temperature. Through a low-pass frequency filtering of the detected spectrum, the wavelength shift of the two patterns can be measured allowing the discrimination of strain and temperature effects with resolutions of 0.45 degrees C and 4.02 mu epsilon, respectively. The sensor is also characterized for angle measurements showing a maximum sensitivity of 9.17 pm/degrees in the range from 0 degrees to 90 degrees. It is demonstrated that with this sensing structure is possible to obtain simultaneous measurement of bend angle and temperature with resolutions of 1.69 degrees and 0.92 degrees C, respectively.
2015
Autores
Hierro Rodriguez, A; Rocha Rodrigues, P; Valdes Bango, F; Alameda, JM; Jorge, PAS; Santos, JL; Araujo, JP; Teixeira, JM; Guerreiro, A;
Publicação
JOURNAL OF PHYSICS D-APPLIED PHYSICS
Abstract
In the present study, we have determined the intrinsic refractive index of anodic aluminium oxide, which is originated by the formation of nanoporous alumina templates. Different templates have been fabricated by the conventional two-step anodization procedure in oxalic acid. Their porosities were modified by chemical wet etching allowing the tuning of their effective refractive indexes (air-filled nanopores + anodic aluminium oxide). By standard spectroscopic light transmission measurements, the effective refractive index for each different template was extracted in the VIS-NIR region. The determination of the intrinsic anodic aluminium oxide refractive index was performed by using the Maxwell-Garnett homogenization theory. The results are coincident for all the fabricated samples. The obtained refractive index (similar to 1.55) is quite lower (similar to 22%) than the commonly used Al2O3 handbook value (similar to 1.75), showing that the amorphous nature of the anodic oxide structure strongly conditions its optical properties. This difference is critical for the correct design and modeling of optical plasmonic metamaterials based on anodic aluminium oxide nanoporous templates.
2015
Autores
Moayyed, H; Leite, IT; Coelho, L; Santos, JL; Viegas, D;
Publicação
24TH INTERNATIONAL CONFERENCE ON OPTICAL FIBRE SENSORS
Abstract
Optical fiber optrodes are attractive sensing devices due to their ability to perform point measurement in remote locations. Mostly, they are oriented to biochemical sensing, quite often relying on fluorescent and spectroscopic techniques, but with the refractometric approach being also considered when the objective is high measurement performance, particularly when focusing on measurand resolution. In this work, we address this subject proposing and theoretically analyzing the characteristics of a fiber optic optrode relying on plasmonic interaction. The optrode structure is a fiber optic tapered tip layout incorporating a lateral bimetallic layer (silver + gold) and operating in reflection.
2015
Autores
Coelho, L; de Almeida, JMMM; Santos, JL; Viegas, D;
Publicação
APPLIED OPTICS
Abstract
A study of a sensor for hydrogen (H-2) detection based on fiber Bragg gratings coated with palladium (Pd) with self-temperature compensation is presented. The cladding around the gratings was reduced down to 50 mu m diameter by a chemical etching process. One of the gratings was left uncoated, and the other was coated with 150 nm of Pd. It was observed that palladium hydride has unstable behavior in environments with high humidity level. A simple solution to overcome this problem based on a Teflon tape is presented. The sensing device studied was able to respond to H-2 concentrations in the range 0%-1% v/v at room temperature and atmospheric pressure, achieving sensitivities larger than 20 pm/% v/v. Considering H-2 concentrations in nitrogen up to 1%, the performance of the sensing head was characterized for different thicknesses of Pd coating ranging from 50 to 200 nm. (C) 2015 Optical Society of America
2015
Autores
Viveiros, D; Ribeiro, J; Ferreira, J; Pinto, AMR; Perez Herrera, RA; Diaz, S; Lopez Gil, A; Dominguez Lopez, A; Esteban, O; Martins, HF; Martin Lopez, S; Baierl, H; Auguste, JL; Jamier, R; Rougier, S; Santos, JL; Flores, D; Roy, P; Gonzalez Herraez, M; Lopez Amo, M; Baptista, JM;
Publicação
PROCEEDINGS OF 2015 3RD EXPERIMENT AT INTERNATIONAL CONFERENCE (EXP AT'15)
Abstract
Coal has been for centuries a central energy source to fulfill industrial and domestic needs. Its large scale extraction produced huge amount of debris that were piled in the neighboring of the mines, quite often going into combustion triggered by events like forest fires or lightning. When in this state it can continue for years, releasing substantial emissions of toxic and greenhouse gases with recognized impact in the environment and, more serious in the short term, in the life quality of the populations located nearby. Continuous monitoring of combustion temperature and emission levels of certain gases opens the possibility to plan corrective actions to minimize their negative impact. Optical fiber technology is wellsuited to this purpose and here it is described the main attributes of a fiber optic sensing system projected to gather data on distributed temperature and gas emission in these harsh environments.
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