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Publicações

Publicações por José Almeida

2019

Mach-Zehnder Interferometers Based on Long Period Fiber Grating Coated With Titanium Dioxide for Refractive Index Sensing

Autores
Soares Guedes Vasconcelos, HCASG; Marques Martins de Almeida, JMMM; Teixeira Saraiva, CMT; da Silva Jorge, PAD; Costa Coelho, LCC;

Publicação
JOURNAL OF LIGHTWAVE TECHNOLOGY

Abstract
The wavelength sensitivity and spectral resolution of Mach-Zehnder fiber interferometers obtained through a combination of two identical uncoated and titanium dioxide (TiO2) coated long period fiber gratings (LPFGs) is presented and compared with single LPFGs-based refractometric sensors. A set of LPFGs were fabricated in single mode fiber with the resonance band having an amplitude of 3 dB in order to split in half the optical power between the core and the specific cladding modes. The separation between the pair of LPFG written in the fiber was varied between 1 and 3 cm and the thickness of the TiO2 coating around the fiber ranged from 20 to 40 nm. A wavelength shift sensitivity of 216 nm/refractive index units (RIU) was achieved for the device with 3 cm and a 30-nm thick TiO2 coating, which presented a spectral resolution of 1.1 x 10(-4 )Rill Despite the lower wavelength shift sensitivity of 142 nm/RIU, attained for a 2-cm long device and 30-nm thick TiO2 coating, a spectral resolution of 1.8 x 10(-5) RIU was measured, which is one order of magnitude lower than a single LPFG.

2019

A Simple Spectral Interrogation System for Optical Fiber Sensors

Autores
Santos,; Jorge,; Almeida,; Coelho,;

Publicação
Proceedings

Abstract
Optical fiber sensors (OFS) based on long-period fiber gratings (LPFG) or on surface plasmon resonance (SPR) represent attractive solutions for detection systems in remote areas. An interrogation system consisting on wavelength modulation of fiber coupled distributed feedback (DFB) lasers was implemented and tested. The system uses a single photodetector to individually acquire the intensity of each DFB laser modulated by the OFS and the real transmission spectrum is reconstructed through curve fitting. Testing was accomplished by measuring the spectral features of an LPFG when changing the surrounding refractive index and errors lower than 1.8 nm in the 1530 to 1570 nm wavelength region were obtained.

2019

Alkali-silica reaction in concrete: Mechanisms, mitigation and test methods

Autores
Figueira, RB; Sousa, R; Coelho, L; Azenha, M; de Almeida, JM; Jorge, PAS; Silva, CJR;

Publicação
CONSTRUCTION AND BUILDING MATERIALS

Abstract
In the last few decades, the alkali-silica reaction (ASR) has been reported as one of the major concrete concerns regarding durability, leading to high maintenance and reconstruction costs. The occurrence of ASR in numerous concrete infrastructures all over the world points to the need for research regarding measures for its detection in an initial stage (and further mitigation) either in new or existing structures. Furthermore, the chemical and physical mechanisms for ASR remain poorly understood. This lack of knowledge leads to incapacity to assess risk, cost-effectively predict service life, and efficiently mitigate the deterioration process due to ASR in concrete structures. This manuscript aims to review the most recent and relevant achievements and the existing knowledge concerning the reaction mechanisms of ASR. Additionally, this manuscript is focused on the conditioning factors, diagnostic and prognostic methodologies, preventive measures and test methods (including their limitations) of ASR conducted at an academic level. The perspectives for future research challenges are also identified and debated.

2017

THE ANTIMICROBIAL EFFECT OF ESSENTIAL OILS AGAINST LISTERIA MONOCYTOGENES IN SOUS VIDE COOK-CHILL BEEF DURING STORAGE

Autores
Gouveia, AR; Alves, M; de Almeida, JMMM; Monteiro Silva, F; Gonzalez Aguilar, G; Silva, JA; Saraiva, C;

Publicação
JOURNAL OF FOOD PROCESSING AND PRESERVATION

Abstract
Sous vide cook-chill (SVCC) is characterized by vacuum-packaging raw or partially prepared foods before pasteurization, followed by rapid chilling and storage below 3C. The application of essential oils (EOs) to food products is a suitable strategy to control pathogens and to extend their shelf life by reducing microbial levels and oxidative processes. The aim of this study was to evaluate the efficacy of Rosmarinus officinalis L. (rosemary) and Thymus vulgaris L. (thyme) EOs against Listeria monocytogenes ATCC 679, inoculated in beef processed by SVCC stored at 2 and 8C for 1, 2, 3, 7, 14, 21 and 28 days. The composition of EOs was identified by gas chromatography-mass spectrometry analysis. The main compounds identified in rosemary EO were eucalyptol (13.05%), camphor (8.93%), verbenone (8.58%), endo-borneol (7.87%) and alpha-pinene (6.78%) and in thyme EO were linalool (18.18%), thymol (7.48%), limonene (6.49%), endo-borneol (5.86%) and terpinen-4-ol (5.66%). Using the minimum inhibitory concentration (MIC) method, L. monocytogenes was inhibited at 3.9 mu L/mL to thyme EO and at 62.5 mu L/mL to rosemary EO. Beef samples of M. longissimus thoracis et lumborum were packaged in bags, inoculated and one of each EO was added at MIC values. Bags were vacuum-sealed and samples were processed at 55C/65 min for 3log(10) CFU/g reduction. A reduction of the counts of L. monocytogenes was observed in all samples at 2C. At 8C counts of L. monocytogenes were almost similar in control samples and those with thyme EO with an increase of themicrobial counts since day 7. Inversely, counts of L. monocytogenes in beef samples with rosemary EO stored at 2 and 8C decreased about 2 log(10) CFU. These results support the possibility of using rosemary EO as natural preservative due to its antimicrobial effect against L. monocytogenes. Also, our results confirm that an adequate chilling storage is essential to guarantee the safety of SVCC product regarding L. monocytogenes to avoid foodborne outbreaks.

2019

Dissolved Carbon Dioxide Sensing Platform for Freshwater and Saline Water Applications: Characterization and Validation in Aquaculture Environments

Autores
Mendes, JP; Coelho, L; Kovacs, B; de Almeida, JMMM; Pereira, CM; Jorge, PAS; Borges, MT;

Publicação
SENSORS

Abstract
A sensing configuration for the real-time monitoring, detection, and quantification of dissolved carbon dioxide (dCO(2)) was developed for aquaculture and other applications in freshwater and saline water. A chemical sensing membrane, based on a colorimetric indicator, is combined with multimode optical fiber and a dual wavelength light-emitting diode (LED) to measure the dCO(2)-induced absorbance changes in a self-referenced ratiometric scheme. The detection and processing were achieved with an embeded solution having a mini spectrometer and microcontroller. For optrode calibration, chemical standard solutions using sodium carbonate in acid media were used. Preliminary results in a laboratory environment showed sensitivity for small added amounts of CO2 (0.25 mg.L-1). Accuracy and response time were not affected by the type of solution, while precision was affected by salinity. Calibration in freshwater showed a limit of detection (LOD) and a limit of quantification (LOQ) of 1.23 and 1.87 mg.L-1, respectively. Results in saline water (2.5%) showed a LOD and LOQ of 1.05 and 1.16 mg.L-1, respectively. Generally, performance was improved when moving from fresh to saline water. Studies on the dynamics of dissolved CO2 in a recirculating shallow raceway system (SRS+RAS) prototype showed higher precision than the tested commercial sensor. The new sensor is a compact and robust device, and unlike other sensors used in aquaculture, stirring is not required for correct and fast detection. Tests performed showed that this new sensor has a fast accurate detection as well as a strong potential for assessing dCO(2) dynamics in aquaculture applications.

2019

Preliminary Study for Detection of Hydrogen Peroxide Using a Hydroxyethyl Cellulose Membrane

Autores
Vasconcelos, H; Almeida, JMMMd; Saraiva, C; Jorge, PAS; Coelho, L;

Publicação
Proceedings

Abstract
High concentration of biogenic amines (BA) is an indicator of deterioration of food and the determination of their concentration is an important method of food control. The hydrogen peroxide (H2O2) is a side product of the degradation of BAs by certain enzymes. It is presented an experimental technique grounded on chemiluminescence to measure small quantities of H2O2 with concentrations as low as 0.01%w/w up to 0.08%w/w. Luminol and cobalt hydroxide are added to hydroxyethyl cellulose to obtain an active membrane which will react with the sampling solution and the amount of total light emission is directly related to the H2O2 concentration.

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