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Publicações

Publicações por CRAS

2016

Characterization of zinc oxide coated optical fiber long period gratings with improved refractive index sensing properties

Autores
Coelho, L; Viegas, D; Santos, JL; de Almeida, JMMM;

Publicação
SENSORS AND ACTUATORS B-CHEMICAL

Abstract
A fiber-optic refractive index (RI) sensor based on a long period fiber grating (LPFG) coated with a zinc oxide (ZnO) thin film was fabricated and characterized. A method to overcoat the LPFG's with a homogeneous ZnO thin films was developed. Characterization of ZnO thin films, deposited simultaneously on silicon (Si) planar substrates, was performed using Scanning Electron Microscope, Energy Dispersive X-ray Spectroscopy and X-ray Photoelectron Spectroscopy. The LPFGs with ZnO coatings from 29 to 145 nm of thickness were characterized and compared in terms of the wavelength shift and the intensity of the attenuation bands changing the surrounding refractive index (SRI) from 1.300 to 1.600. An average wavelength sensitivity of similar to 7162 nm/RIU was achieved in the RI range from 1.440 to 1.456 and more than 12,000 nm/RIU at 1.440 RI. Using a ZnO film thickness of 116 nm and in the RI region between 1.320 and 1.360 the average sensitivity of similar to 806 nm/RIU was measured for a 145 nm thick film. Working as an intensity sensing device, the 87 nm coated LPFG shows a linear sensitivity of 216.4 dB/RIU in a wide range of RI from 1.340 to 1.420.

2016

Fabrication and Characterization of Metal Oxide-Coated Long-Period Fiber Gratings

Autores
Coelho, L; Santos, JL; Viegas, D; Marques Martins de Almeida, JMMM;

Publicação
JOURNAL OF LIGHTWAVE TECHNOLOGY

Abstract
Sensors based on long-period fiber gratings (LPFGs) over coated with metal oxide were fabricated and characterized for refractive index (RI) sensing. Oxidation of Ni, Ti, Al, and Cr was monitored in real time by following the features of the LPFG attenuation band. Themetals were deposited simultaneously on top of Si substrates for further chemical and morphological analysis. Wavelength sensitivities (nm/RIU) of about 10 437 at 1.432, 1150 at 1.400, 20 125 at 1.448, and 875 at 1.420 were achieved for LPFGs coated, with 68 nm of Ni, 60 nm of TiO2, 50 nm of Al2O3, and 62 nm of Cr2O3, respectively. For surrounding RI higher than the cladding RI, the wavelength sensitivities are 1937, 6801, 5762, and 3051 nm/RIU at 1.457 for the Ni, Ti, Al, and Cr oxides, respectively. Working as intensity sensing devices sensitivities up to 167 dB/RIU were measured. Metal oxide coated LPFGs leads to wavelength sensitivity enhancement comparing to bare LPFGs and may be used in systems with RI higher than the fiber cladding, a region where bare LPFGs are insensitive.

2016

Optical sensor based on hybrid FBG/titanium dioxide coated LPFG for monitoring organic solvents in edible oils

Autores
Coelho, L; Viegas, D; Santos, JL; de Almeida, JMMM;

Publicação
TALANTA

Abstract
A hybrid optical sensing scheme based on a fiber Bragg grating (FBG) combined with a titanium dioxide coated long period fiber grating (LPFG) for monitoring organic solvents in high refractive index edible oils is reported. In order to investigate and optimize the sensor performance, two different FBG/LPFG interrogation systems were investigated. The readout of the sensor was implemented using either the wavelength shift of the LPFG resonance dip or the variation in the optical power level of the reflected/transmitted light at the FBG wavelength peak, which in turn depends on the wavelength position of the LPFG resonance. Hexane concentrations up to 20%V/V, corresponding to the refractive index range from 1.451 to 1.467, were considered. For the transmission mode of operation, sensitivities of 1.41 nm/%V/V and 0.11 dB/%V/V, with resolutions of 0.58%V/V and 0.29%V/V, were achieved when using the LPFG wavelength shift and the FBG transmitted optical power, respectively. For the FBG reflection mode of operation, a sensitivity of 0.07 dB/V/V and a resolution better than 0.16%V/V were estimated.

2016

Analysis of a Plasmonic Based Optical Fiber Optrode With Phase Interrogation

Autores
Moayyed, H; Leite, IT; Coelho, L; Santos, JL; Viegas, D;

Publicação
PHOTONIC SENSORS

Abstract
Optical fiber optrodes are attractive sensing devices due to their ability to perform point measurement in remote locations. Mostly, they are oriented to biochemical sensing, quite often supported by fluorescent and spectroscopic techniques, but with the refractometric approach considered as well when the objective is of high measurement performance, particularly when the focus is on enhancing the measurand resolution. In this work, we address this subject, proposing and analyzing the characteristics of a fiber optic optrode relying on plasmonic interaction. A linearly tapered optical fiber tip is covered by a double overlay: the inner one - a silver thin film and over it a dielectric layer, with this combination allowing to achieve, at a specific wavelength range, surface plasmonic resonance (SPR) interaction sensitive to the refractive index of the surrounding medium. Typically, the interrogation of the SPR sensing structures is performed, considering spectroscopic techniques, but in principle, a far better performance can be obtained, considering the reading of the phase of the light at a specific wavelength located within the spectral plasmonic resonance. This is the approach which is studied here in the context of the proposed optical fiber optrode configuration. The analysis performed shows the combination of a silver inner layer with a dielectric titanium oxide layer with tuned thicknesses enables sensitive phase reading and allows the operation of the fiber optic optrode sensor in the third telecommunication wavelength window.

2016

Zinc oxide coated optical fiber long period gratings for sensing of volatile organic compounds

Autores
Coelho, L; Viegas, D; Santos, JL; de Almeida, JMMM;

Publicação
OPTICAL SENSING AND DETECTION IV

Abstract
The detection of volatile organic compounds is accomplished with a sensing device based on a long period fiber grating (LPFG) coated with a zinc oxide (ZnO) thin layer with self-temperature compensation. The ZnO coating structure was produced onto the cladding of the fiber by thermal oxidation of a metallic Zn thin film. The morphological characterization of ZnO thin films, grown at the same time on silicon substrates, was performed using X-ray diffraction, X-ray Photoelectron Spectroscopy and Scanning Electron Microscope which shows very good agreement. LPFGs with 290 nm thick ZnO coating were fabricated and characterized for the detection of ethanol and hexane in vapor phase. For ethanol a sensitivity of 0.99 nm / g.m(-3) was achieved when using the wavelength shift interrogation mode, while for hexane a much lower sensitivity of 0.003 nm / g.m(-3) was measured, indicating a semi-selectivity of the sensor with a spectral resolution better than 3.2 g.m(-3).

2016

Combining coastal geoscience mapping and photogrammetric surveying in maritime environments (Northwestern Iberian Peninsula): focus on methodology

Autores
Pires, A; Chamine, HI; Piqueiro, F; Perez Alberti, A; Rocha, F;

Publicação
ENVIRONMENTAL EARTH SCIENCES

Abstract
Digital photogrammetry and GIS-based mapping are increasingly recognised as powerful tools in littoral issues. This paper considers the interoperability framework for high-resolution imagery acquisition and the development of coastal geoscience maps. The layered system architecture of the cartographic methodology is also explained. Moreover, it highlights a new approach to assessing heterogeneous geologic, geomorphological and maritime environments. The main goal of the present study was to test a new concept for photogrammetric images in order to assist modelling techniques, spatial analysis and coastal conceptual models. This approach proposes a methodological approach to coastal zone monitoring and to maritime forcing conditions evaluating. This approach will allow: (1) the acquisition of a large archive of high-resolution imagery; (2) the development of a coastal database including the entire data field and in situ assessments; (3) the study of coastal dynamics and shoreline evolution; (4) the assessment of the rock platforms and hydraulic structures; (5) the production of coastal geosciences maps. An integrated coastal geoscience and engineering methodology was outlined in NW of Iberian Peninsula (South Galicia and North/Central Portugal regions). This paper reports on the increased knowledge of the studied regions, providing essential data concerning coastal geo-morphodynamics. The overall assessment revealed additional evidence of erosion issues, which contributes to a better understanding of the hydraulic conditions. The main results are presented in regional coastal geoscience maps and local approach-outputs that could help government, local authorities and stakeholders to develop coastal management plans and to recommend strategies.

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